Testing by Vanguard Laboratory · Olympia, Washington360-967-7010

Wastewater chemistry

EPA 160.4: Volatile solids

Scope EPA 160.4 for volatile solids. Define sample matrix, preparation, reporting limits and project requirements.

Volatile solids measurement context

EPA Method 160.4: the residue from a total, dissolved or suspended solids test is ignited at 550 °C, and the weight lost is the volatile solids, a rough measure of organic matter. Tell us which residue the result should be based on. Reported as mg/L.

Connect the parameter to the sample plan

Specify grab or composite collection where applicable, the reporting unit and any field or preparation requirements. Keep nitrogen, phosphorus, solids and demand measurements on their correct reporting basis.

Include the complete project requirement

Provide the matrix, target analytes, required method, fraction, units and reporting limits. Include the permit or monitoring instructions where results will support a regulatory submission. Naming this method does not establish blanket compliance eligibility.

Resolve collection before sampling

Use the bottle, preservation and delivery instructions assigned to the agreed scope. Identify each location and collection time, and document any deviation. The final analytical plan must fit the submitted material and its intended use.

Related testing & guidance

Technical & service references

Vanguard service details

Source review: November 8, 2026. The agreed method and project scope govern the testing.

Start with a defined scope

Build a project scope

Tell us the sample, the question and the decision your results need to support.

Build a testing request